Optimization of ultrasonic-assisted extraction of polysaccharides from Ulva rigida and evaluation of their antioxidant activity
Yazarlar (3)
Azat Akbal
Central Research Institute of Food And Feed Control, Türkiye
Saliha Şahin Bursa Uludağ Üniversitesi, Türkiye
Prof. Dr. Betül GÜROY Yalova Üniversitesi, Türkiye
Makale Türü Özgün Makale (SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
Dergi Adı Algal Research (Q1)
Dergi ISSN 2211-9264 Dergi Bilgileri (2024)
Dergi Tarandığı Indeksler SCI
Makale Dili İngilizce Basım Tarihi 01-2024
Cilt / Sayı / Sayfa 77 / 1 / 103356– DOI 10.1016/j.algal.2023.103356
Makale Linki https://doi.org/10.1016/j.algal.2023.103356
UAK Araştırma Alanları
Sucul Biyoteknoloji
Özet
Ultrasonic-assisted extraction (UAE) of sulfated polysaccharides from the cell walls of Ulva rigida green macroalgae was performed with a central composite design using the independent variables (pH 2–10, extraction temperature 40–80 °C, time 50–130 min and liquid/solid ratio of raw material 15–75 mL/g) with response surface methodology. Optimum conditions were obtained as pH 4.92, extraction temperature 73 °C, time 126 min, and the liquid/solid ratio of the raw material as 68 mL/g. Under these optimum conditions, the experimental yield was obtained as 13.22 %, and the results were close and in harmony with the estimated value of 12.91 %. FT-IR results, especially at the peaks corresponding to wave numbers 850 cm−1 and 1256 cm−1, the tension vibrations of sulfated esters in C-O-S and Ssingle bondO bonds were more clearly observed in the extracted ulvan components. As a result of the SEM …
Anahtar Kelimeler
Antioxidant activity | Central composite design | Extracted sulfated polysaccharides | Ulva rigida